Synthesis and examination of new PVA-Fe2O3-Au hybrid composite

Mohammed, Kahtan A.; Abdul Kareem, Alyaa Abdul Hasan; Judi, Hawraa K.; Rathan, Athota; Algburi, Sameer; Alkhafaji, Mohammed Ayad; Zabibah, Rahman S.

doi:10.47176/ijpr.23.3.41674

Synthesis and examination of new PVA-Fe2O3-Au hybrid composite

Document Type : Original Article

Authors

Kahtan A. Mohammed ¹

Alyaa Abdul Hasan Abdul Kareem ²

Hawraa K. Judi ³

Athota Rathan ⁴

Sameer Algburi ⁵

Mohammed Ayad Alkhafaji ⁶

Rahman S. Zabibah ⁷

¹ Department of Medical Physics,Faculty of Medical Sciences, Jabir Ibn Hayyan Medical University, Najaf, 54001, Iraq

² Department of chemistry and polymer research, polymer research center, University of Basrah, Basrah, Iraq

³ 3. Department of medical physics, Hilla University College, Babylon, Iraq

⁴ Department of Aeronautical engineering, Institute of Aeronautical, Hyderabad, Telangana, India

⁵ Computer Engineering Techniques Department, College of Engineering Techniques, Al-Kitab University, Altun Kupri, Kirkuk, Iraq

⁶ National University of Science and Technology, Dhi Qar, Iraq

⁷ Medical Laboratory Technology Department, College of Medical Technology, the Islamic University, Najaf, Iraq

https://doi.org/10.47176/ijpr.23.3.41674

Abstract

In current work, new hybrid composite have been prepared by mixing gold nanocolloid physically with PVA-Fe₂O₃. Morphological, compositional, structure and optical properties of hybrid composites were studied by transmission electron microscope (TEM), scanning electron microscope (SEM), energy dispersive spectroscopy (EDS), Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD) and UV-visible spectroscopy (UV-VIS). XRD results showed that both Au and Fe2O3 have peaks in the structure and that confirmed by EDS and FTIR results. Microscopes results indicated the nanosized nature of prepared materials. UV–vis spectrum show absorption edge at 440 nm which relates to PVA-Fe2O3 mixed with Au which means there is a red shift after incorporation of Au in the composites. And the energy gap of composite became equal to 2.48 eV after adding Au solution.

Keywords

Fe2O3

nanocomposite

hybrid materials

Subjects

Nanomaterials

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